4CDJ

Structure of ZNRF3 ectodomain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Detector	DECTRIS PILATUS
Spacegroup name	P 1 21 1
Unit cell lengths	35.686, 73.503, 58.573
Unit cell angles	90.00, 97.49, 90.00

Refinement procedure

Resolution	45.567 - 1.500
R-factor	0.1625
Rwork	0.162
R-free	0.17730
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.018
RMSD bond angle	1.842
Data reduction software	XDS
Data scaling software	Aimless
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall
Low resolution limit [Å]	45.570
High resolution limit [Å]	1.500
Rmerge	0.020
Number of reflections	46197
<I/σ(I)>	24.1
Completeness [%]	96.6
Redundancy	2.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1				0.2 M AMMONIUM FORMATE AT PH 6.6 WITH 20% W/V PEG3350