4C9V
Xenopus RNF43 ectodomain in complex with Xenopus RSPO2 Fu1-Fu2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-07-09 |
| Detector | DECTRIS PILATUS |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 88.847, 35.841, 87.876 |
| Unit cell angles | 90.00, 114.58, 90.00 |
Refinement procedure
| Resolution | 32.780 - 2.700 |
| R-factor | 0.32048 |
| Rwork | 0.317 |
| R-free | 0.39456 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.748 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 32.760 |
| High resolution limit [Å] | 2.700 |
| Rmerge | 0.150 |
| Number of reflections | 6845 |
| <I/σ(I)> | 9.4 |
| Completeness [%] | 95.8 |
| Redundancy | 3.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
