4C9D
Cas6 (TTHB231) product complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-04-14 |
Detector | ADSC |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 75.220, 75.220, 308.780 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 73.083 - 3.000 |
R-factor | 0.246 |
Rwork | 0.244 |
R-free | 0.29070 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4c98 |
RMSD bond length | 0.005 |
RMSD bond angle | 0.942 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 73.080 | 3.080 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.130 | 0.780 |
Number of reflections | 18676 | |
<I/σ(I)> | 16.6 | 2.8 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 7.7 | 8.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 0.1M TRIS (PH 8.5), 13% (W/V) PEG 65 20000 |