4C8A
mouse ZNRF3 ectodomain crystal form II
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-02-22 |
| Detector | ADSC CCD |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 71.284, 76.454, 89.331 |
| Unit cell angles | 90.00, 93.26, 90.00 |
Refinement procedure
| Resolution | 52.150 - 2.700 |
| R-factor | 0.22726 |
| Rwork | 0.224 |
| R-free | 0.29852 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.518 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 52.090 | |
| High resolution limit [Å] | 2.700 | 2.700 |
| Rmerge | 0.060 | |
| Number of reflections | 13223 | |
| <I/σ(I)> | 20.6 | |
| Completeness [%] | 99.5 | |
| Redundancy | 9.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
