4C1N
Corrinoid protein reactivation complex with activator
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.2 |
Synchrotron site | BESSY |
Beamline | 14.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-12-15 |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | P 1 |
Unit cell lengths | 67.134, 128.175, 163.366 |
Unit cell angles | 77.61, 82.25, 88.76 |
Refinement procedure
Resolution | 30.631 - 2.530 |
R-factor | 0.1934 |
Rwork | 0.191 |
R-free | 0.24290 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.003 |
RMSD bond angle | 0.740 |
Phasing software | PHENIX |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.600 |
High resolution limit [Å] | 2.530 | 2.530 |
Rmerge | 0.090 | 0.540 |
Number of reflections | 168978 | |
<I/σ(I)> | 10 | 2.6 |
Completeness [%] | 96.0 | 85 |
Redundancy | 2.74 | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |