4C0W

The crystal strucuture of native PpAzoR

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-4
Synchrotron site	ESRF
Beamline	ID14-4
Temperature [K]	100
Detector technology	CCD
Detector	ADSC QUANTUM 315r
Spacegroup name	F 2 2 2
Unit cell lengths	72.299, 95.743, 146.539
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	26.130 - 1.600
R-factor	0.1541
Rwork	0.153
R-free	0.17930
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.010
RMSD bond angle	1.280
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall
Low resolution limit [Å]	53.700
High resolution limit [Å]	1.600
Rmerge	0.050
Number of reflections	33249
<I/σ(I)>	13.9
Completeness [%]	99.1
Redundancy	4.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7	293	4% PEG 400, 2M AMMONIUM SULPHATE, 0.1M HEPES PH 7.0 AT 293K