4BSO
Crystal structure of R-spondin 1 (Fu1Fu2) - Native
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 37.160, 63.900, 92.460 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.480 - 2.200 |
R-factor | 0.2139 |
Rwork | 0.212 |
R-free | 0.24990 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.021 |
RMSD bond angle | 2.124 |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 34.400 |
High resolution limit [Å] | 2.200 |
Rmerge | 0.100 |
Number of reflections | 5873 |
<I/σ(I)> | 11.1 |
Completeness [%] | 100.0 |
Redundancy | 7.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |