4BM5

Chloroplast inner membrane protein TIC110

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSRRC BEAMLINE BL13B1
Synchrotron site	NSRRC
Beamline	BL13B1
Temperature [K]	100
Detector technology	CCD
Detector	ADSC CCD
Spacegroup name	P 65 2 2
Unit cell lengths	121.100, 121.100, 242.400
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	27.370 - 4.200
R-factor	0.35
Rwork	0.350
R-free	0.36600
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.011
RMSD bond angle	2.500
Data scaling software	SCALEPACK
Refinement software	CNS (1.3)

Data quality characteristics

	Overall
Low resolution limit [Å]	30.000
High resolution limit [Å]	4.200
Rmerge	0.100
Number of reflections	8171
<I/σ(I)>	27.8
Completeness [%]	99.7
Redundancy	12.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1