4BH7
CRYSTAL STRUCTURE OF GERMLINE ANTIBODY 36-65 IN COMPLEX WITH PEPTIDE PPYPAWHAPGNI
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 2006-05-13 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 54.560, 76.770, 59.170 |
Unit cell angles | 90.00, 102.31, 90.00 |
Refinement procedure
Resolution | 57.810 - 2.890 |
R-factor | 0.22993 |
Rwork | 0.227 |
R-free | 0.25419 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2a6j |
RMSD bond length | 0.015 |
RMSD bond angle | 1.804 |
Data reduction software | MOSFLM |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 57.000 | 3.050 |
High resolution limit [Å] | 2.890 | 2.890 |
Rmerge | 0.120 | 0.320 |
Number of reflections | 10548 | |
<I/σ(I)> | 9.4 | 3.9 |
Completeness [%] | 97.8 | 99.7 |
Redundancy | 4.7 | 4.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 0.05 M SODIUM CACODYLATE PH 6.5, 18% PEG 3000 |