4BFM

The crystal structure of mouse PK38

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE BL-17A
Synchrotron site	Photon Factory
Beamline	BL-17A
Temperature [K]	100
Detector technology	CCD
Detector	ADSC QUANTUM 4r
Spacegroup name	P 21 21 21
Unit cell lengths	35.799, 75.711, 128.088
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	48.896 - 2.350
R-factor	0.1767
Rwork	0.175
R-free	0.20820
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3ZGW
RMSD bond length	0.009
RMSD bond angle	1.213
Data scaling software	HKL-2000
Phasing software	MOLREP
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.390
High resolution limit [Å]	2.400	2.350
Rmerge	0.100	0.360
Number of reflections	15230
<I/σ(I)>	35.78	6.21
Completeness [%]	99.8	99.1
Redundancy	10.8	7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1