4BE8
NEDD4 HECT A889F structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-12-10 |
Detector | DECTRIS PILATUS 2M |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 100.545, 100.545, 96.450 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 44.580 - 2.996 |
R-factor | 0.2482 |
Rwork | 0.246 |
R-free | 0.29500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2xbb |
RMSD bond length | 0.003 |
RMSD bond angle | 0.787 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.580 | 3.100 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.070 | 0.700 |
Number of reflections | 11622 | |
<I/σ(I)> | 28.4 | 3.9 |
Completeness [%] | 99.3 | 99.1 |
Redundancy | 13 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 9 | 1.15 M POTASSIUM SODIUM TARTRATE, 0.1 M TRIS-HCL, PH 9.0 |