4BDU
Bax BH3-in-Groove dimer (GFP)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-05-25 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | P 64 |
Unit cell lengths | 112.314, 112.314, 293.270 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.959 - 2.998 |
R-factor | 0.2165 |
Rwork | 0.215 |
R-free | 0.24600 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.390 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.900 | 3.100 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.173 | 1.731 |
Number of reflections | 41413 | |
<I/σ(I)> | 17.74 | 2.26 |
Completeness [%] | 99.5 | 95.7 |
Redundancy | 20.7 | 17.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 10% PEG3350, 20% MPD, 0.5% CHAPS, 0.1 M TRIS PH 8.0 |