4B3D
Humanised monomeric RadA in complex with 5-methyl indole
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-03-15 |
Detector | ADSC QUANTUM 210 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 40.280, 87.246, 62.628 |
Unit cell angles | 90.00, 91.50, 90.00 |
Refinement procedure
Resolution | 40.266 - 1.589 |
R-factor | 0.1803 |
Rwork | 0.179 |
R-free | 0.21200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1PZN CHAIN A |
RMSD bond length | 0.006 |
RMSD bond angle | 0.982 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | AMoRE |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.620 | 1.690 |
High resolution limit [Å] | 1.590 | 1.590 |
Rmerge | 0.060 | 0.610 |
Number of reflections | 57763 | |
<I/σ(I)> | 13.76 | 2.19 |
Completeness [%] | 99.2 | 96.5 |
Redundancy | 3.7 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.2 | 8% PEG-1000, 100 MM NAK PHOSPHATE, PH 6.2 |