4B0Z
Crystal structure of S. pombe Rpn12
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-03-17 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.780, 91.380, 143.340 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.111 - 1.585 |
R-factor | 0.1898 |
Rwork | 0.188 |
R-free | 0.22480 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.015 |
RMSD bond angle | 1.525 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHELX |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.340 | 1.670 |
High resolution limit [Å] | 1.590 | 1.590 |
Rmerge | 0.050 | 0.500 |
Number of reflections | 74706 | |
<I/σ(I)> | 17.1 | 2.5 |
Completeness [%] | 99.7 | 99.7 |
Redundancy | 3.9 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 0.2 M NA NO3, 0.1 M BIS-TRIS PROPANE PH 7.5, 22.5% PEG3350 |