4AYV

Human thrombin - inhibitor complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	ELLIOTT GX-21
Temperature [K]	15
Detector technology	AREA DETECTOR
Collection date	1993-10-22
Detector	MULTIWIRE XENTRONICS
Wavelength(s)	1.5418
Spacegroup name	P 43 21 2
Unit cell lengths	90.800, 90.800, 132.500
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	24.510 - 2.800
R-factor	0.14299
Rwork	0.141
R-free	0.19209
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.009
RMSD bond angle	1.382
Data reduction software	XDS
Data scaling software	XDS
Refinement software	REFMAC (5.7.0025)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.800
Rmerge	0.050
Number of reflections	12962
Redundancy	2.29

Crystallization Conditions

crystal ID	method	pH	temperature	details
1