4ANO
Crystal Structure Geobacillus thermodenitrificans EssB cytoplasmic fragment
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2010-02-13 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 74.622, 74.622, 83.545 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.610 - 1.700 |
R-factor | 0.20777 |
Rwork | 0.205 |
R-free | 0.25262 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.023 |
RMSD bond angle | 2.009 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.610 | 1.790 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.050 | 0.460 |
Number of reflections | 26751 | |
<I/σ(I)> | 24.4 | 4.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 9.6 | 7.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 0.1 M TRI-SODIUM CITRATE PH5.5, 20% PEG3000, 0.25MM TRIS(2-CARBOXYETHYL)PHOSPHINE HYDROCHLORIDE |