Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-1 |
| Synchrotron site | ESRF |
| Beamline | ID14-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-07-23 |
| Detector | ADSC QUANTUM 210 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 132.197, 109.677, 176.332 |
| Unit cell angles | 90.00, 97.11, 90.00 |
Refinement procedure
| Resolution | 15.000 - 2.050 |
| R-factor | 0.20755 |
| Rwork | 0.206 |
| R-free | 0.23992 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1JXA CHAIN A |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.828 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.090 |
| High resolution limit [Å] | 2.050 | 2.050 |
| Rmerge | 0.080 | 0.720 |
| Number of reflections | 151822 | |
| <I/σ(I)> | 16.75 | 2 |
| Completeness [%] | 98.6 | 97.2 |
| Redundancy | 5.45 | 4.62 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | 3% PEG 400, 0.1 M HEPES PH 7.5, 0.8 M LICL, 0.01 M FRUCTOSE-6P |
