4AJ7
Crystallographic structure of thioredoxin from Litopenaeus vannamei (oxidized form).
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X6A |
| Synchrotron site | NSLS |
| Beamline | X6A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-12-08 |
| Detector | ADSC CCD |
| Spacegroup name | P 32 1 2 |
| Unit cell lengths | 57.895, 57.895, 117.869 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 19.094 - 2.035 |
| R-factor | 0.1768 |
| Rwork | 0.174 |
| R-free | 0.22490 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3zzx |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.066 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 19.640 | 2.150 |
| High resolution limit [Å] | 2.040 | 2.040 |
| Rmerge | 0.060 | 0.240 |
| Number of reflections | 14756 | |
| <I/σ(I)> | 3.1 | 3.1 |
| Completeness [%] | 99.4 | 96.6 |
| Redundancy | 6.4 | 4.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4.6 | 2.0 M AMMONIUM SUPHATE, 0.1 M SODIUM ACETATE, PH 4.6 |
