4AI6
Dynein Motor Domain - ADP complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-4 |
| Synchrotron site | ESRF |
| Beamline | ID14-4 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC QUANTUM 315 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 174.886, 119.175, 193.974 |
| Unit cell angles | 90.00, 90.18, 90.00 |
Refinement procedure
| Resolution | 49.290 - 3.400 |
| R-factor | 0.24453 |
| Rwork | 0.241 |
| R-free | 0.30300 |
| Structure solution method | SAD |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.557 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Refinement software | REFMAC (5.7.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.200 | 3.700 |
| High resolution limit [Å] | 3.400 | 3.400 |
| Rmerge | 0.120 | |
| Number of reflections | 109899 | |
| <I/σ(I)> | 19.4 | 2.6 |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 21.8 | 21.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
