4ABM
Crystal Structure of CHMP4B hairpin
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-4 |
| Synchrotron site | ESRF |
| Beamline | ID14-4 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 37.590, 71.430, 123.680 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 61.860 - 1.800 |
| R-factor | 0.23043 |
| Rwork | 0.228 |
| R-free | 0.28517 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.018 |
| RMSD bond angle | 0.884 |
| Data scaling software | iMOSFLM |
| Phasing software | SHELX |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 41.230 | 1.900 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Rmerge | 0.270 | 0.410 |
| Number of reflections | 30007 | |
| <I/σ(I)> | 16.3 | 4.4 |
| Completeness [%] | 99.6 | 100 |
| Redundancy | 7.8 | 7.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
