4A9A
Structure of Rbg1 in complex with Tma46 dfrp domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-11-05 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 86.200, 224.890, 84.890 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 56.220 - 2.670 |
R-factor | 0.19655 |
Rwork | 0.196 |
R-free | 0.22212 |
Structure solution method | SIRAS |
Starting model (for MR) | NONE |
RMSD bond length | 0.007 |
RMSD bond angle | 1.233 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHARP |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 79.420 | 2.820 |
High resolution limit [Å] | 2.670 | 2.670 |
Rmerge | 0.080 | 0.400 |
Number of reflections | 47671 | |
<I/σ(I)> | 6.5 | 1.9 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 7.14 | 7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 2.38 SODIUM FORMATE, 0.2-0.25 SODIUM CITRATE PH 6.5 |