4A4X
NEK2-EDE bound to CCT248662
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 101.223, 56.909, 74.408 |
| Unit cell angles | 90.00, 127.12, 90.00 |
Refinement procedure
| Resolution | 50.379 - 2.400 |
| R-factor | 0.2065 |
| Rwork | 0.204 |
| R-free | 0.24690 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.597 |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.380 |
| High resolution limit [Å] | 2.400 |
| Rmerge | 0.110 |
| Number of reflections | 13251 |
| <I/σ(I)> | 7.5 |
| Completeness [%] | 99.4 |
| Redundancy | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
