4A4K
Crystal structure of the S. cerevisiae Ski2 insertion domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-07-31 |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 230.463, 123.139, 153.201 |
Unit cell angles | 90.00, 131.05, 90.00 |
Refinement procedure
Resolution | 57.159 - 3.250 |
R-factor | 0.237 |
Rwork | 0.236 |
R-free | 0.25650 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.001 |
RMSD bond angle | 0.354 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 96.000 | 3.430 |
High resolution limit [Å] | 3.250 | 3.250 |
Rmerge | 0.090 | 0.660 |
Number of reflections | 50807 | |
<I/σ(I)> | 8.4 | 1.5 |
Completeness [%] | 99.6 | 99.9 |
Redundancy | 2.9 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 3.5 M SODIUM FORMATE, 0.1 M MES PH 6.5 |