4A4J
Crosstalk between Cu(I) and Zn(II) homeostasis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-05-30 |
Detector | ADSC CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 22.780, 58.040, 24.780 |
Unit cell angles | 90.00, 112.82, 90.00 |
Refinement procedure
Resolution | 29.020 - 1.250 |
R-factor | 0.14476 |
Rwork | 0.143 |
R-free | 0.17988 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2xmw |
RMSD bond length | 0.011 |
RMSD bond angle | 1.421 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 22.840 | 1.320 |
High resolution limit [Å] | 1.250 | 1.250 |
Rmerge | 0.050 | 0.260 |
Number of reflections | 15818 | |
<I/σ(I)> | 13.6 | 4.2 |
Completeness [%] | 96.2 | 87.5 |
Redundancy | 3.3 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 100 MM HEPES PH 7.5 10% PEG 4000 5% ISOPROPANOL |