4A4A
CpGH89 (E483Q, E601Q), from Clostridium perfringens, in complex with its substrate GlcNAc-alpha-1,4-galactose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 113 |
Spacegroup name | P 61 |
Unit cell lengths | 90.996, 90.996, 252.856 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 78.810 - 1.900 |
R-factor | 0.17103 |
Rwork | 0.169 |
R-free | 0.21003 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.017 |
RMSD bond angle | 1.483 |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 1.900 |
Rmerge | 0.080 |
Number of reflections | 92199 |
<I/σ(I)> | 9.7 |
Completeness [%] | 99.4 |
Redundancy | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |