4A3O
Crystal structure of the USP15 DUSP-UBL monomer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 31 |
Unit cell lengths | 100.419, 100.419, 71.704 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 55.324 - 2.200 |
R-factor | 0.2023 |
Rwork | 0.201 |
R-free | 0.22940 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3pv1 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.001 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.030 | 2.320 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.090 | 0.420 |
Number of reflections | 61255 | |
<I/σ(I)> | 8 | 2.3 |
Completeness [%] | 99.0 | 96.5 |
Redundancy | 2.9 | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 1.9 M (NH4)2SO4, 100 MM HEPES PH 7.0, 200 MM KI |