4A0P
Crystal structure of LRP6P3E3P4E4
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 169.815, 42.699, 119.879 |
| Unit cell angles | 90.00, 97.49, 90.00 |
Refinement procedure
| Resolution | 29.090 - 1.900 |
| R-factor | 0.18284 |
| Rwork | 0.181 |
| R-free | 0.21098 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1ijq |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.099 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.950 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rmerge | 0.100 | 0.560 |
| Number of reflections | 66493 | |
| <I/σ(I)> | 9.4 | 2 |
| Completeness [%] | 98.0 | 88.4 |
| Redundancy | 4.1 | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
