431D
5'-D(*GP*GP*CP*CP*AP*AP*TP*TP*GP*G)-3'
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ELETTRA BEAMLINE 5.2R |
Synchrotron site | ELETTRA |
Beamline | 5.2R |
Temperature [K] | 120 |
Detector technology | IMAGE PLATE |
Collection date | 1996-05-23 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 26.106, 36.455, 52.559 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.150 |
R-factor | 0.167 * |
Starting model (for MR) | UDJ049 USED AS STARTING MODEL FOR REFINEMENT |
RMSD bond length | 0.017 |
Data reduction software | DENZO |
Data scaling software | CCP4 ((SCALA)) |
Refinement software | SHELXL-93 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 1.180 |
High resolution limit [Å] | 1.150 | 1.150 |
Rmerge | 0.054 | 0.158 |
Total number of observations | 63114 * | |
Number of reflections | 17760 | |
<I/σ(I)> | 25 | 11.71 |
Completeness [%] | 96.7 | 95 * |
Redundancy | 3.6 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 6 | 289. * | pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 289.0K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | SODIUM CACODYLATE | ||
2 | 1 | 1 | MGCL2 | ||
3 | 1 | 1 | SPERMINE | ||
4 | 1 | 1 | MPD | ||
5 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | oligonucleotide | 0.41 (mM) | ||
2 | 1 | buffer | 10.6 (mM) | ||
5 | 1 | 1 | spermine | 0.22 (mM) | |
6 | 1 | 2 | MPD | 40 (%) |