418D
5'-R(*GP*UP*GP*CP*AP*CP*A)-D(P*C)-3'
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | SIEMENS |
| Temperature [K] | 291 |
| Detector technology | AREA DETECTOR |
| Detector | NICOLET |
| Spacegroup name | I 21 21 21 |
| Unit cell lengths | 24.290, 45.250, 73.680 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.400 |
| R-factor | 0.208 |
| Rwork | 0.208 |
| R-free | 0.25900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | R(GUAUAUA)DC |
| RMSD bond length | 0.004 |
| RMSD bond angle | 1.800 |
| Data reduction software | X-GEN |
| Data scaling software | X-GEN |
| Phasing software | AMoRE |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.400 |
| Rmerge | 0.042 |
| Number of reflections | 1314 |
| Completeness [%] | 72.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | pH 7.00 |
