418D
5'-R(*GP*UP*GP*CP*AP*CP*A)-D(P*C)-3'
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | SIEMENS |
Temperature [K] | 291 |
Detector technology | AREA DETECTOR |
Detector | NICOLET |
Spacegroup name | I 21 21 21 |
Unit cell lengths | 24.290, 45.250, 73.680 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.400 |
R-factor | 0.208 |
Rwork | 0.208 |
R-free | 0.25900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | R(GUAUAUA)DC |
RMSD bond length | 0.004 |
RMSD bond angle | 1.800 |
Data reduction software | X-GEN |
Data scaling software | X-GEN |
Phasing software | AMoRE |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.400 |
Rmerge | 0.042 |
Number of reflections | 1314 |
Completeness [%] | 72.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | pH 7.00 |