414D
5'-D(*GP*GP*GP*GP*CP*GP*CP*CP*CP*C)-3'
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 291 |
Detector technology | IMAGE PLATE |
Collection date | 1996-12-15 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 45.504, 46.084, 28.465 |
Unit cell angles | 90.00, 100.74, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.900 |
R-factor | 0.174 * |
RMSD bond length | 0.005 |
RMSD bond angle | 32.800 * |
Data reduction software | MAR |
Data scaling software | XDS |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 10.000 |
High resolution limit [Å] | 1.800 |
Rmerge | 0.062 |
Total number of observations | 41278 * |
Number of reflections | 10033 |
Completeness [%] | 92.4 |
Redundancy | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 6.5 | 291 * | pH 6.50, VAPOR DIFFUSION, HANGING DROP, temperature 293.00K |
1 | Vapor diffusion, sitting drop * | 6.5 | 291 * | pH 6.50, VAPOR DIFFUSION, HANGING DROP, temperature 293.00K |
1 | Vapor diffusion, sitting drop * | 6.5 | 291 * | pH 6.50, VAPOR DIFFUSION, HANGING DROP, temperature 293.00K |
1 | Vapor diffusion, sitting drop * | 6.5 | 291 * | pH 6.50, VAPOR DIFFUSION, HANGING DROP, temperature 293.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | SODIUM CACODYLATE | ||
2 | 1 | 1 | MGCL2 | ||
3 | 1 | 1 | SPERMINE | ||
4 | 1 | 1 | MPD | ||
5 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | DNA | 2 (mM) | |
2 | 1 | drop | sodium cacodylate | 20 (mM) | |
3 | 1 | drop | 30 (mM) | ||
4 | 1 | drop | spermine tetrachloride | 2 (mM) | |
5 | 1 | drop | 5 (%) | ||
6 | 1 | reservoir | MPD | 50 (%) |