3ZZP
Circular permutant of ribosomal protein S6, lacking edge strand beta- 2 of wild-type S6.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I911-2 |
Synchrotron site | MAX II |
Beamline | I911-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-03-13 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 22.200, 40.800, 68.660 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 0.960 |
R-factor | 0.1129 |
R-free | 0.13690 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ris |
RMSD bond length | 0.016 |
RMSD bond angle | 0.033 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 0.990 |
High resolution limit [Å] | 0.960 | 0.960 |
Rmerge | 0.060 | 0.650 |
Number of reflections | 38300 | |
<I/σ(I)> | 16 | 3 |
Completeness [%] | 99.3 | 98.2 |
Redundancy | 6 | 4.86 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 1.9M AMMONIUM SULPHATE, 0.1M MES PH 6.5, 8% 1,4 DIOXANE |