3ZYO
Crystal structure of the N-terminal leucine rich repeats and immunoglobulin domain of netrin-G ligand-3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-08-05 |
Detector | ADSC CCD |
Spacegroup name | H 3 2 |
Unit cell lengths | 131.330, 131.330, 174.870 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.600 - 3.100 |
R-factor | 0.23044 |
Rwork | 0.229 |
R-free | 0.26931 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3zyn |
RMSD bond length | 0.005 |
RMSD bond angle | 0.857 |
Data reduction software | HKL-2000 |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.600 | 3.270 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmerge | 0.130 | 0.870 |
Number of reflections | 10743 | |
<I/σ(I)> | 11.2 | 2.6 |
Completeness [%] | 99.9 | 100 |
Redundancy | 7.3 | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 0.1 M NAH2PO4, 0.1 M KH2PO4, 2M NACL, 0.1 M MES, PH 6.5 |