3ZYH
CRYSTAL STRUCTURE OF PA-IL LECTIN COMPLEXED WITH GALBG0 AT 1.5 A RESOLUTION
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-06-02 |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 40.559, 72.865, 133.723 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.264 - 1.501 |
R-factor | 0.1863 |
Rwork | 0.185 |
R-free | 0.20150 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1l7l |
RMSD bond length | 0.005 |
RMSD bond angle | 1.108 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 66.860 | 1.590 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.030 | 0.070 |
Number of reflections | 61876 | |
<I/σ(I)> | 34.5 | 14.8 |
Completeness [%] | 96.1 | 84.2 |
Redundancy | 3.5 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 293 | 1.5 M AMMONIUM SULFATE AND 0.1 M SODIUM ACETATE PH 4.6. |