3ZYB
CRYSTAL STRUCTURE OF PA-IL LECTIN COMPLEXED WITH GALAG0 AT 2.3 A RESOLUTION
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-08-20 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 53.332, 128.559, 146.063 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.261 - 2.290 |
R-factor | 0.2151 |
Rwork | 0.214 |
R-free | 0.24040 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1l7l |
RMSD bond length | 0.002 |
RMSD bond angle | 0.691 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 73.070 | 2.430 |
High resolution limit [Å] | 2.290 | 2.290 |
Rmerge | 0.100 | 0.440 |
Number of reflections | 45434 | |
<I/σ(I)> | 10 | 2.8 |
Completeness [%] | 98.8 | 93.5 |
Redundancy | 3.63 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 3.5 | 0.1 M CITRIC ACID PH 3.5 AND 25% W/V POLYETHYLENE GLYCOL 3350 |