3ZX7
Complex of lysenin with phosphocholine
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-04-18 |
Detector | MARRESEARCH |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 98.110, 98.110, 184.170 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 23.700 - 2.840 |
R-factor | 0.2255 |
Rwork | 0.224 |
R-free | 0.26400 |
Structure solution method | MIRAS |
Starting model (for MR) | NONE |
RMSD bond length | 0.009 |
RMSD bond angle | 1.110 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | SHARP |
Refinement software | BUSTER (2.11.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.100 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.100 | 0.800 |
Number of reflections | 12994 | |
<I/σ(I)> | 29 | 4.9 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 22.1 | 23 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.5 | 1.8 M AMMONIUM DI-HYDROGEN PHOSPHATE, 1.0 M SODIUM ACETATE PH 4.5 |