3ZVZ
PHD finger of human UHRF1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 1 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 1 |
| Temperature [K] | 110 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 51.006, 51.006, 83.629 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 24.394 - 1.449 |
| R-factor | 0.1705 |
| Rwork | 0.169 |
| R-free | 0.19720 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.155 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 24.400 | 1.450 |
| High resolution limit [Å] | 1.430 | 1.430 |
| Rmerge | 0.090 | 0.480 |
| Number of reflections | 20810 | |
| <I/σ(I)> | 19.3 | 2.1 |
| Completeness [%] | 92.2 | 54.7 |
| Redundancy | 3.7 | 1.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
