3ZVR
Crystal structure of Dynamin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-04-17 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 178.450, 191.610, 60.520 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 95.805 - 3.100 |
R-factor | 0.2153 |
Rwork | 0.212 |
R-free | 0.27200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2AKA CHAIN B PDB ENTRY 2DYN CHAIN B PDB ENTRY 3LJB CHAIN B |
RMSD bond length | 0.008 |
RMSD bond angle | 1.098 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE: 1.7.1_743)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 95.800 | 3.180 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmerge | 0.070 | 0.880 |
Number of reflections | 18735 | |
<I/σ(I)> | 15.4 | 1.9 |
Completeness [%] | 96.7 | 66.2 |
Redundancy | 4.1 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.7 | 52.5 MM TRIS.HCL PH 7.7, 175 MM NACL, 32.5 MM NANO3, 20 % V/V PEG 400, 0.97 MM BETA-MERCAPTOETHANOL, 31.9 MICROM DYN1 G397D DELTA PRD |