3ZUO
OMCI in complex with leukotriene B4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 120 |
Detector technology | CCD |
Collection date | 2008-07-26 |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 41.756, 112.789, 62.394 |
Unit cell angles | 90.00, 101.89, 90.00 |
Refinement procedure
Resolution | 61.060 - 1.860 |
R-factor | 0.2209 |
Rwork | 0.220 |
R-free | 0.23790 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3zui |
RMSD bond length | 0.006 |
RMSD bond angle | 0.870 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 112.790 | 1.960 |
High resolution limit [Å] | 1.860 | 1.860 |
Rmerge | 0.030 | 0.500 |
Number of reflections | 46060 | |
<I/σ(I)> | 17.7 | 2.1 |
Completeness [%] | 96.9 | 82.6 |
Redundancy | 2.6 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.4 | 21% PEG 4000, 0.2 M SODIUM ACETATE, TRIS 0.1 M PH 8.4. |