3ZTM
Cytochrome c prime from alcaligenes xylosoxidans: as isolated L16G variant at 0.9 A resolution: unrestraint refinement
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-05-10 |
Detector | ADSC CCD |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 53.377, 53.377, 181.652 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 0.900 |
R-factor | 0.133 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2yl7 |
RMSD bond length | 0.016 |
RMSD bond angle | 2.138 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | REFMAC |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 0.920 |
High resolution limit [Å] | 0.900 | 0.900 |
Rmerge | 0.070 | 0.590 |
Number of reflections | 115947 | |
<I/σ(I)> | 33 | 3.3 |
Completeness [%] | 98.3 | 83 |
Redundancy | 9.9 | 6.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | AMMONIUM SULPHATE, TRIS PH 7.5. |