3ZTH
Crystal structure of Stu0660 of Streptococcus thermophilus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X12C |
Synchrotron site | NSLS |
Beamline | X12C |
Temperature [K] | 93 |
Detector technology | CCD |
Collection date | 2011-03-29 |
Detector | ADSC QUANTUM 210 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 118.149, 101.869, 102.784 |
Unit cell angles | 90.00, 115.14, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.400 |
R-factor | 0.2046 |
Rwork | 0.205 |
R-free | 0.24310 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.006 |
RMSD bond angle | 1.300 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | autoSHARP |
Refinement software | CNS (1.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.440 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.080 | 0.250 |
Number of reflections | 80761 | |
<I/σ(I)> | 27.8 | 3.4 |
Completeness [%] | 98.9 | 97 |
Redundancy | 5.6 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | pH 7 |