3ZT9
The bacterial stressosome: a modular system that has been adapted to control secondary messenger signaling
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-11-25 |
Detector | ADSC CCD |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 42.000, 46.920, 87.770 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.476 - 1.750 |
R-factor | 0.1538 |
Rwork | 0.152 |
R-free | 0.18860 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.016 |
RMSD bond angle | 1.500 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | SHELXDE |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.480 | 1.790 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.070 | 0.340 |
Number of reflections | 19966 | |
<I/σ(I)> | 10.5 | 3.1 |
Completeness [%] | 99.8 | 100 |
Redundancy | 5.1 | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 1 UL PROTEIN, 1 UL CRYSTALLANT, 1 ML WELL, 14 % PEG 3350, 0.2 M NACL, 0.1 M BIS-TRIS PH 5.5. |