3ZS6
The Structural characterization of Burkholderia pseudomallei OppA.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-04-05 |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 46.860, 81.930, 74.180 |
Unit cell angles | 90.00, 104.34, 90.00 |
Refinement procedure
Resolution | 38.464 - 2.100 |
R-factor | 0.1602 |
Rwork | 0.158 |
R-free | 0.20880 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1qka |
RMSD bond length | 0.006 |
RMSD bond angle | 0.909 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.970 | 2.210 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.090 | 0.290 |
Number of reflections | 31801 | |
<I/σ(I)> | 13.2 | 5.6 |
Completeness [%] | 100.0 | 99.9 |
Redundancy | 4.5 | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.1 M HEPES PH 7.5, 20% PEG 8000. |