3ZQW
Structure of CBM3b of major scaffoldin subunit ScaA from Acetivibrio cellulolyticus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-02-23 |
Detector | MARRESEARCH |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 52.506, 52.506, 193.978 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.616 - 1.070 |
R-factor | 0.1219 |
Rwork | 0.121 |
R-free | 0.13520 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.011 |
RMSD bond angle | 1.403 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHELX (C D E) |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.100 |
High resolution limit [Å] | 1.080 | 1.080 |
Rmerge | 0.080 | 0.650 |
Number of reflections | 69264 | |
<I/σ(I)> | 24.4 | 1.8 |
Completeness [%] | 98.9 | 97.2 |
Redundancy | 17.57 | 9.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 1.9 M AMMONIUM SULFATE, 0.1 M HEPES PH 7.5, 0.5% (W/V) POLYETHYLENE GLYCOL 400. | ||
1 | 7.5 | 1.9 M AMMONIUM SULFATE, 0.1 M HEPES PH 7.5, 0.5% (W/V) POLYETHYLENE GLYCOL 400. |