3ZPN
Structure of Psb28
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-07-21 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 43 |
Unit cell lengths | 57.060, 57.060, 183.320 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 57.060 - 2.361 |
R-factor | 0.1945 |
Rwork | 0.193 |
R-free | 0.23420 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2kvo |
Data reduction software | XDS |
Data scaling software | TRUNCATE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 57.060 | 2.420 |
High resolution limit [Å] | 2.360 | 2.360 |
Rmerge | 0.050 | 0.760 |
Number of reflections | 23633 | |
<I/σ(I)> | 13.26 | 1.52 |
Completeness [%] | 98.7 | 97.6 |
Redundancy | 3.12 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 35% W/V PEG 3350, 300MM POTASSIUM THIOCYANATE |