Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL11-1 |
| Synchrotron site | SSRL |
| Beamline | BL11-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | MARMOSAIC 325 mm CCD |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 50.820, 68.530, 58.900 |
| Unit cell angles | 90.00, 112.35, 90.00 |
Refinement procedure
| Resolution | 20.390 - 1.550 |
| R-factor | 0.1889 |
| Rwork | 0.187 |
| R-free | 0.21570 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2GOZ |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.945 |
| Data reduction software | iMOSFLM |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.390 | 1.630 |
| High resolution limit [Å] | 1.550 | 1.550 |
| Rmerge | 0.030 | 0.630 |
| Number of reflections | 26462 | |
| <I/σ(I)> | 13.9 | |
| Completeness [%] | 97.6 | 99.6 |
| Redundancy | 3 | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 1.7M SODIUM MALONATE, PH 7.5 AND 1 MM MGCL2 |
