3ZOY
Crystal Structure of N64Del Mutant of Nitrosomonas europaea Cytochrome c552 (hexagonal space group)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-04-04 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 137.668, 137.668, 88.830 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 119.220 - 2.300 |
R-factor | 0.17732 |
Rwork | 0.175 |
R-free | 0.22570 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3zox |
RMSD bond length | 0.029 |
RMSD bond angle | 2.027 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 68.800 | 2.400 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.160 | 0.570 |
Number of reflections | 22416 | |
<I/σ(I)> | 9 | 3.7 |
Completeness [%] | 99.5 | 99.6 |
Redundancy | 5.6 | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 0.1 M TRIS-HCL PH 8.5, 3.1 M AMMONIUM SULFATE |