3ZLE
Crystal structure of Toxoplasma gondii sporozoite AMA1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARMOSAIC 325 mm CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 179.190, 155.520, 180.590 |
Unit cell angles | 90.00, 92.31, 90.00 |
Refinement procedure
Resolution | 78.040 - 2.350 |
R-factor | 0.21044 |
Rwork | 0.209 |
R-free | 0.24393 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2x2z |
RMSD bond length | 0.013 |
RMSD bond angle | 1.310 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 79.300 | 2.480 |
High resolution limit [Å] | 2.350 | 2.350 |
Rmerge | 0.080 | 0.340 |
Number of reflections | 391285 | |
<I/σ(I)> | 10 | 2.1 |
Completeness [%] | 95.4 | 75.8 |
Redundancy | 3.6 | 2.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 1.0 M SUCCINIC ACID PH 7.0, 100 MM HEPES PH 7.0, 1% PEG MONOMETHYL ETHER 2000 AND 100 MM GLYCINE |