3ZLD
Crystal structure of Toxoplasma gondii sporozoite AMA1 in complex with a 36 aa region of sporozoite RON2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARMOSAIC 325 mm CCD |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 49.370, 124.180, 171.910 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 85.960 - 3.100 |
R-factor | 0.2109 |
Rwork | 0.205 |
R-free | 0.26334 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ZLE CHAIN A |
RMSD bond length | 0.011 |
RMSD bond angle | 1.221 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 85.960 | 3.270 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmerge | 0.110 | 0.310 |
Number of reflections | 9716 | |
<I/σ(I)> | 8.2 | 3.5 |
Completeness [%] | 97.8 | 95.8 |
Redundancy | 4 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.2 M MAGNESIUM CHLORIDE HEXAHYDRATE, 0.1 M HEPES PH 7.5, 25% PEG3350 |