3ZK0
The crystal structure of a Cu(I) metallochaperone from Streptomyces lividans in its apo form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-05-02 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.600, 47.680, 48.950 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.160 - 1.700 |
R-factor | 0.18561 |
Rwork | 0.183 |
R-free | 0.23303 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3zja |
RMSD bond length | 0.015 |
RMSD bond angle | 1.771 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.160 | 1.790 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.090 | 0.440 |
Number of reflections | 11478 | |
<I/σ(I)> | 8.8 | 1.9 |
Completeness [%] | 98.0 | 89.5 |
Redundancy | 3.9 | 2.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 31 % PEG 8K, 0.2 M SODIUM ACETATE AND 0.1 M SODIUM CACODYLATE, PH 6.5 |