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3ZJV

Ternary complex of E .coli leucyl-tRNA synthetase, tRNA(Leu) and the benzoxaborole AN3213 in the editing conformation

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID14-2
Synchrotron siteESRF
BeamlineID14-2
Temperature [K]100
Detector technologyCCD
Collection date2008-07-09
DetectorADSC QUANTUM 4
Spacegroup nameP 1 21 1
格子定数 [Å]89.370, 76.940, 90.710
格子定数 [度]90.00, 102.37, 90.00
精密化法
残基88.740 - 2.310
R因子0.20282
Rwork0.200
R-free0.24747
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1h3n
結合長の平均二乗偏差(RMSD) [Å]0.012
結合角の平均二乗偏差(RMSD) [度]1.458
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHASER
Refinement softwareREFMAC (5.6.0111)
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)88.7002.370
分解能 [Å] (高)2.3102.310
Rmerge_l_obs0.0600.580
独立反射数52864
<I/σ(I)>16.82.5
完全性 [%]99.999.9
冗長性3.753.76
結晶化条件
結晶ID方法pH温度溶液条件
15.6THE TERNARY COMPLEX ECLEURS-TRNA-AN3213 WAS CRYSTALLIZED FROM 0.1 M SODIUM ACETATE AT PH 5.6, 14-18 % PEG 6000 AND 200 MM NACL. CRYSTALS WERE FROZEN IN LIQUID NITROGEN USING A CRYOPROTECTING SOLUTION CONTAINING 22 % ETHYLENE GLYCOL

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件を2024-09-18に公開中

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